XH-300UP Microwave Ultrasonic Ultraviolet Combined Catalytic Synthesis System

The XH-300UP Computerized Microwave-Ultrasonic-UV Combined Catalytic Synthesis System supplied by Guangzhou Jincheng Scientific Instrument Co., Ltd. features three modes: microwave, ultrasonic, and ultraviolet light, along with microwave hydrothermal functionality. It enables microwave hydrothermal reaction systems at different scales, representing a new generation of combined instruments that perfectly integrate electromagnetic waves, sound waves, and light waves.

The combined ultrasonic-UV catalytic synthesis system utilizes the thermal and non-thermal effects of microwaves to reduce molecular activation energy; employs the cavitation and mechanical effects of ultrasound to accelerate solute dissolution, with immense energy concentration during cavitation bubble collapse; and uses UV irradiation to cause internal electrons to undergo energy level transitions upon photon absorption, forming unstable excited states that further dissociate or undergo other reactions. Since absorption of photons at specific wavelengths is often characteristic of certain molecular groups, photocatalysis provides the optimal means to induce reactions at specific molecular sites. In summary, this instrument significantly accelerates chemical reaction rates through these physical and chemical processes, enabling reactions that do not occur under conventional conditions or enhancing existing reaction speeds and extents, thereby opening new reaction pathways.

Features:

The control system of the combined ultrasonic-UV catalytic synthesis system adopts the latest Android operating system, equipped with a quad-core 1.2GHz processor and 16GB storage. Combined with an 8-inch color LCD touch display, it allows real-time photography and video recording of the reaction process, which can be exported to a computer for data analysis. Parameters such as ultrasonic power and duty cycle, microwave power, temperature, pressure, and time can be set in stages. The ultrasonic transducer is enclosed and not exposed outside the instrument, nor can it be directly pulled out from the top of the chamber, avoiding safety hazards. Synergistic control technology, combined with constant temperature and constant power modes, maximizes the advantages of different energy fields such as microwave, ultrasonic, and UV, and systematically integrates them to deliver diverse effects in catalysis, organic/inorganic synthesis, natural product/mineral extraction, and nanomaterial preparation.

Technical Specifications:

1. The combined ultrasonic-UV catalytic synthesis system supports both microwave atmospheric and microwave high-pressure reaction modes; it allows synergistic combination or individual operation of microwave, ultrasonic, and UV, as an integrated unit without external power supply;

2. Microwave frequency: 2450MHz; Microwave output power: 0~1000W continuously adjustable;

3. Ultrasonic frequency: 25±1KHz; Ultrasonic output power: 0~1500W continuously adjustable; Ultrasonic pulse duty cycle: arbitrarily adjustable; Ultrasonic transducer features automatic frequency search, maintaining maximum acoustic power even when reactant properties and viscosity change;

4. UV wavelength: 365nm; UV output power: 250W;

5. UV irradiation intensity probe measurement range: 0.1~1.999×10⁵ μW/cm², displayed in real-time on the instrument; stray light in the UV out-of-band region: UV365 <0.02%;

6. Unique synergistic combination control technology, combined with constant temperature and constant power modes, maximizes the advantages of different energy fields such as microwave, ultrasonic, and UV, and systematically integrates them to deliver diverse effects in catalysis, organic/inorganic synthesis, natural product/mineral extraction, and nanomaterial preparation;

7. Large-volume resonant cavity made of austenitic non-magnetic stainless steel, integrally pressed, with a one-piece bottom steel plate, offering excellent corrosion resistance and microwave reflection properties;

8. High-precision contact PT1000 temperature sensor, rapid heating, atmospheric temperature control range: 0~300°C, high-pressure temperature control range: 0~260°C, temperature measurement accuracy: ±0.1°C; temperature control accuracy: ±1°C;

9. Pressure monitoring system, real-time monitoring of pressure changes in the reaction system; pressure control begins when set pressure is reached, pressure control range: 0~6MPa, maximum pressure tolerance: 10MPa, pressure measurement accuracy: 0.01MPa, detection frequency: 150~200 data points/second;

10. Dual temperature and pressure control; real-time data acquisition via temperature and pressure sensors; control is activated upon reaching either target temperature or target pressure first, ensuring safety; the system includes over-temperature and over-pressure protection.

11. High-pressure reactor volume: 100ml; medium-pressure reactor volume: 250ml; low-pressure reactor volume: 500ml;

12. High-pressure reactor pressure control range: 0~6MPa, maximum working pressure ≥6MPa; medium-pressure reactor pressure control range: 0~4MPa; low-pressure reactor pressure control range: 0~2MPa;

13. Control system uses the latest Android operating system, quad-core 1.2GHz processor, 2GB RAM, 16GB storage, USB interface; real-time display of ultrasonic power, microwave power, temperature, pressure, time, and graphs; the instrument can set up to 20 reaction stages and store unlimited reaction data sets and experimental methods;

14. 8-inch color LCD touch display, 12-megapixel camera for real-time photography and video recording of the reaction process;

15. USB interface allows insertion of a USB drive to export historical experimental data for playback and analysis on a computer via配套 software; also allows export of images and videos captured by the built-in camera.

16. Powerful magnetic stirring system, speed: 1400r/min, applicable to both high-pressure and atmospheric systems; stirring speed is continuously adjustable and displays real-time speed;

17. Remote control device for emergency shutdown from a distance;

18. Configurable with inert gas protection interface; open reaction system, allowing installation of dropping funnel and condenser for reflux reactions;

19. Microwave leakage complies with national standards.

Technical Parameters:

Information about the Computerized Microwave-Ultrasonic-UV Combined Catalytic Synthesis System is provided by Guangzhou Jincheng Scientific Instrument Co., Ltd. For more details about the photocatalytic synthesis system, please feel free to contact us.