AL-HSR12 Type Rolling Microwave Hydrothermal Synthesis Apparatus

Instrument Introduction:

The AL-HSR12 Rolling Microwave Hydrothermal Synthesizer provides a fast and automated solution for samples, accelerating the synthesis reaction speed under high-pressure conditions. It is suitable for the synthesis of nanomaterials, inorganic materials, and high-temperature pressure-resistant systems, widely used in research institutes, universities, and other units.

Features:

The instrument adopts microwave non-pulse continuous automatic frequency conversion control, extending the service life of the instrument and ensuring the uniformity of electromagnetic waves. The cavity is specially made of 85L large-capacity 316L stainless steel material. The self-locking buffering explosion-proof furnace door ensures the safety of the operator and the integrity of the furnace door structure in case of abnormal reactions. The furnace door and cavity are tightly sealed, with microwave leakage complying with national standards. The instrument uses a dual-control system for temperature and pressure to monitor and display the synthesis experiment in real-time. 360° continuous rotation ensures uniform microwave distribution, guaranteeing the same microwave environment for all samples and improving the consistency of experimental results.

The rolling rotation method places the reaction vessels horizontally, ensuring uniform mixing of reactants inside the vessels.

When the pressure inside the vessel exceeds the set protection value, the microwave heating automatically stops. The explosion-proof membrane has a dual safety function: if the pressure exceeds the membrane's capacity, it ruptures first to release gas, preventing damage to the vessel and ensuring operator safety.

Technical Parameters:

*1. Power output mode: Microwave power automatically adjusts with temperature via frequency conversion control, providing non-pulse continuous heating.

2. Output power: 3000W, automatically and continuously adjustable.

*3. Upper power limit can be set arbitrarily, with a lower power limit function to ensure continuous power output.

*4. Three temperature control modes: heating to the set temperature with upper power limit followed by insulation mode; rate heating mode for slow heating by reaching the set temperature over a set time; and heating slope mode with set temperature increase per minute.

5. High-precision platinum resistance temperature sensor, temperature control range: -50~300°C; temperature control accuracy: ±0.5°C; includes rate heating function required for hydrothermal synthesis.

6. Maximum operating temperature: 260°C.

7. Pressure control range: 0~4MPa, pressure sensor range: 0~10MPa, maximum pressure resistance: 10MPa, pressure control accuracy: 0.01MPa.

*8. 360° continuous rolling rotation ensures uniform microwave distribution, guaranteeing the same microwave environment for all samples and improving the consistency of experimental results.

*9. Capable of continuous uninterrupted operation.

*10. 7-inch touch screen LCD display with touch operation, real-time display of temperature, pressure, and power in the sealed reaction vessel, along with temperature, pressure, and power curves. Includes functions for saving and querying experimental records.

11. 85L large-capacity 316L stainless steel cavity with 6 layers of corrosion-resistant PFA Teflon coating. Resistant to corrosion and high temperatures.

12. 200ml microwave synthesis vessel, with the outer vessel made of imported PEEK glass fiber aerospace material and the inner vessel made of TFM material.

*13. Main vessel connected to temperature and pressure sensors; auxiliary vessel uses a double-vent pressure release screw with an explosion-proof membrane. Ceramic material remains stable without deformation at high temperatures.

14. High-throughput sample synthesis, capable of synthesizing up to 12 samples simultaneously or individually from 1 to 12 samples.

15. Rolling rotation method places the reaction vessels horizontally, ensuring uniform mixing of reactants inside the vessels.

*16. 10-inch touch control panel for remote wireless operation, with a resolution of 1280*800, IPS screen type, and real-time synchronization with the touch control screen.

*17. Control panel performance: 64-bit Win11 operating system, Intel quad-core CPU, 8GB RAM, 128GB storage. Supports WiFi, Bluetooth, 3.5mm audio interface, dual Type-C ports, speakers, microphone, and HD camera.

18. Self-locking explosion-proof furnace door ensures operator safety and structural integrity in case of abnormal reactions.

19. The furnace cavity is equipped with a high-power exhaust system that continuously cools the reaction vessels. Exhaust volume is not less than 5m³/min.

*20. Utilizes AI artificial intelligence logic algorithms to achieve accurate control of complex, long-lag objects, ensuring precise temperature control and eliminating overheating or underheating phenomena.

21. Microwave leakage complies with national standards.

*Note: Items marked with an asterisk are the technological advantages of our company's products.