AL-MUUHC03 Microwave Ultrasonic Ultraviolet Hydrothermal Synthesis Combined Reactor

Instrument Introduction:

The AL-MUUHC03 Microwave-Ultrasonic-Ultraviolet Hydrothermal Synthesis Combined Reactor is a product designed based on our company's control technology and tailored to the needs of university faculty and students. This instrument features eight experimental modes: microwave, ultrasonic, ultraviolet, microwave-ultrasonic combination, microwave-ultraviolet combination, ultrasonic-ultraviolet combination, microwave-ultrasonic-ultraviolet combination, and microwave hydrothermal synthesis reaction. It is a combined synthesis instrument that integrates electromagnetic waves, sound waves, light waves, and hydrothermal synthesis.

Utilizes the thermal and non-thermal effects of microwaves;

Employs ultrasonic cavitation and mechanical action to accelerate solute dissolution, with immense energy concentration during cavitation bubble collapse;

Uses ultraviolet irradiation to cause molecules to absorb photons, leading to internal electron energy level transitions, forming unstable excited states that further dissociate or undergo other reactions. Since the absorption of photons of a specific wavelength is often characteristic of a particular molecular group, photocatalysis enables reactions at specific molecular sites.

Leverages high-pressure reaction vessels to accelerate sample synthesis reactions under high-pressure conditions, enabling hydrothermal synthesis reactions suitable for nanomaterials, inorganic materials, and high-temperature pressure-resistant systems.

Accelerates chemical reaction rates through physical and chemical processes, facilitating reactions that would not occur under normal conditions or enhancing existing reaction speeds and degrees.

The high-power immersion ultrasonic transducer operates in environments up to 300°C with a frequency of 25kHz. Key features include precise temperature control, a 7-inch display screen, touch control, simple and convenient operation, and data storage capabilities. The AL-MUUHC03 Microwave-Ultrasonic-Ultraviolet Hydrothermal Synthesis Combined Reactor boasts powerful digital processing functions, real-time online display and recording of reaction data and curve graphs, programmable reaction conditions, the ability to divide experiments into multiple working stages, online modification of unsuitable reaction parameters, and functions for saving and querying experimental records.

The ultrasonic probe of the AL-MUUHC03 Microwave-Ultrasonic-Ultraviolet Hydrothermal Synthesis Combined Reactor is fixed with quick-connect fittings, allowing the probe to be detached and the ultrasonic device to be used separately for other experiments, greatly expanding the instrument's application scenarios. With the quick-connect cover closed, the device can be used solely for microwaves, and the cavity, free from the ultrasonic probe, significantly increases usable space.

The ultraviolet lamp tube of the AL-MUUHC03 Microwave-Ultrasonic-Ultraviolet Hydrothermal Synthesis Combined Reactor has a spectral energy distribution centered at 365nm, with a power of 250W. The top features a cooling fan to reduce the temperature of the ultraviolet lamp tube, and the lamp tube can be easily replaced by the user.

The hydrothermal reaction vessel of the AL-MUUHC03 Microwave-Ultrasonic-Ultraviolet Hydrothermal Synthesis Combined Reactor provides high-pressure conditions to accelerate sample synthesis reactions, making it suitable for the synthesis of nanomaterials, inorganic materials, and high-temperature pressure-resistant systems. It is widely used in research institutions, universities, and other units.

Application Fields:

The AL-MUUHC03 Microwave-Ultrasonic-Ultraviolet Hydrothermal Synthesis Combined Reactor is particularly outstanding for microwave extraction, synthesis, catalysis, and activation of biological macromolecules, proteins, peptides, enzymes, etc., in plant and animal fields, significantly impacting experiments in related areas.

The AL-MUUHC03 Microwave-Ultrasonic-Ultraviolet Hydrothermal Synthesis Combined Reactor can catalyze various types of organic, pharmaceutical, and biochemical reactions, such as addition, substitution, esterification, hydrolysis, alkyl(acyl)ation, polymerization, condensation, cyclization, and oxidation, as well as physical processes like solvent extraction of food, natural products, and minerals. It is applicable to organic synthetic chemistry, pharmaceutical chemistry, food science, quarantine and epidemic prevention, molecular biology, analytical chemistry, inorganic chemistry, petrochemicals, materials science, biomedical science, and other related fields.

Technical Parameters:

1. Three catalytic reaction methods: microwave, ultrasonic, and ultraviolet, combinable into seven experimental modes;

*2. Microwave power: 0-1000W, freely adjustable, with automatic frequency conversion control based on temperature, non-pulse continuous heating.

*3. Upper limit of microwave power freely settable, with a lower power limit function to ensure continuous power output.

*4. Three temperature control modes: heating to set temperature with upper power limit then maintaining temperature, rate heating mode for gradual temperature increase over set time, and heating slope mode with set temperature increase per minute.

5. Ultrasonic power: 0～1200W continuously adjustable; ultrasonic frequency: 25±1KHz;

6. Automatic frequency search and lock function for ultrasonic frequency, maintaining optimal power despite changes in reactant properties and viscosity;

7. Ultrasonic operating environment: 0～300℃;

8. Ultrasonic probe diameters: Ф10mm, Ф20mm, suitable for different reaction container sizes;

9. Ultraviolet wavelength: 365nm; power: 250W;

*10. Ultraviolet lamp tube equipped with cooling fan at the top for heat dissipation, and user-replaceable aging ultraviolet lamp tubes.

*11. Equipped with E365 ultraviolet intensity detector;

*12. Temperature measurement and control range: 0～300℃; includes rate heating function.

13. Temperature measurement accuracy: ≤±0.2℃; temperature control accuracy: ≤±1℃;

14. Pressure control range: 0~6MPa, pressure sensor range: 0～10MPa, pressure resistance上限15MPa, pressure control accuracy: 0.01MPa;

15. Microwave synthesis vessel volumes: 100ml, 250ml, and 500ml; outer vessel made of imported PEEK aerospace material, inner vessel made of PTFE; magnetic stirring available during experiments.

*16. 35L large-capacity 316L austenitic stainless steel cavity, with high corrosion and temperature resistance;

17. High-precision contact temperature sensor for real-time monitoring of reaction temperature and precise control of reaction progress;

*18. Capable of continuous uninterrupted operation.

*19. 7-inch high-brightness TFT LCD touch screen for direct operation, Cortex-A8 CPU core, equipped with USB interface; real-time display of reaction temperature and power data with curves, capable of saving and querying experimental records;

*20. Built-in high-definition camera, 7-inch monitor for real-time display of reactant changes, with optional video recording.

*21. Equipped with 10-inch tablet for remote wireless control, screen resolution 1280*800, 64-bit Win11 operating system, Intel quad-core CPU, 8GB RAM, 128GB storage; supports WiFi, Bluetooth, 3.5mm audio interface, USB-C interface, speakers, microphone, and high-definition camera.

22. Provides magnetic stirring at various speeds, stepless speed adjustment 0～2000 rpm; mechanical stirring speed range: 0～2000 rpm (optional);

*23. Utilizes AI artificial intelligence logic algorithms for precise temperature control of any substance regardless of properties, enabling accurate control of complex, long-lag objects, preventing overheating or undercooling;

*24. Ultrasonic transducer connected to microwave cavity via quick-connect fittings, allowing separate use of ultrasonic part and microwave part.

25. Reaction volume: 10～2000mL; accommodates 2L reaction flasks or 2L double-jacketed reaction flasks;

*26. Equipped with inert gas protection interface and four liquid inlets/outlets for fluid dynamics experiments;

27. Open reaction system, allowing installation of dropping funnels and condensers for reflux reactions;

28. Cavity equipped with high-power exhaust system, enabling various reactions to proceed continuously in a ventilated, easily observable environment.

29. Microwave leakage complies with national standards.

*Indicates our company's superior technologies.